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Journal of Dental Research, Vol. 82, No. 2, 141-145 (2003)
DOI: 10.1177/154405910308200213

Hybridization Efficiency of the Adhesive/Dentin Interface with Wet Bonding

Y. Wang1 and P. Spencer1,2,*

1 Department of Oral Biology and
2 Department of Pediatric Dentistry, University of Missouri-Kansas City School of Dentistry, 650 E. 25th St., Kansas City, MO 64108;


Figure 1
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Figure 1. Light micrographs and Raman spectra of Single Bond adhesive/dentin interface (a) and Single Bond adhesive-infiltrated demineralized dentin (AIDD) without or with removal of ethanol before polymerization (b, c, respectively). These 3-µm sections were stained with Goldner’s trichrome; corresponding Raman spectra were recorded from the intertubular area of the samples.

 

Figure 2
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Figure 2. Light micrograph (a) and corresponding Raman mapping spectra (b) acquired at 1-µm intervals across the Single Bond adhesive/dentin interface. The spectra marked with arrows (c) were recorded from sites corresponding to the demarcations noted on the light micrograph.

 

Figure 3
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Figure 3. Raman intensity ratios of 1454/1667 (a) and 1113/1667 (b) and penetration of BisGMA monomer and BisGMA/HEMA (c) as a function of spatial position across the adhesive/dentin interface. The comparable relative ratios calculated from the AIDD represent the optimum hybrid and are presented for comparison.

 

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