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J Dent Res 35(1): 16-24, 1956
© 1956 International and American Associations for Dental Research

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THE DETECTION AND ESTIMATION OF RESIDUAL MONOMER IN POLYMETHYL METHACRYLATE

D. C. SMITH 1 and M. E. D. BAINS 1

1 Department of Prosthetics, University of Manchester, England

1. The detection and estimation of residual methyl methacrylate in polymethyl methacrylate has been achieved by physical and chemical methods.

2. A qualitative method in which the aqueous extract of the denture base is tested using a potassium permanganate reagent has been developed.

3. The best quantitative method was found to be a bromination procedure, a method using infrared absorption spectra proving less accurate.

4. The consequences of preliminary results obtained with these methods are briefly discussed.







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